Journal of Environmental Treatment Techniques  
2021, Volume 9, Issue 1, Pages: 172-177  
J. Environ. Treat. Tech.  
ISSN: 2309-1185  
Journal web link: http://www.jett.dormaj.com  
https://doi.org/10.47277/JETT/9(1)183  
Verification of the Effect of Raw Materials Mill Dust  
on Soil Stabilization: An Experimental Study  
1
*
2
1
Fatima Alsaleh , Feras Al Adday , Ahmed Al-Abu Hussein  
1
Department of Transportation Engineering, Faculty of Civil Engineering, University of Aleppo,  
2
Middle East University, Amman, Jordan  
Received: 26/07/2020  
Accepted: 21/10/2020  
Published: 20/03/2021  
Abstract  
Cement plants produce large quantities of dust, which is an important source of pollution. Among these pollutants is raw materials mill  
dust (RMMD), it is a dust produced during the grinding of raw materials. RMMD differs in chemical composition from cement kiln dust  
(
CKD), where CKD is a by-product that collects in the electrostatic filters of a cement kiln. A lot of studies have been done around the world  
to find effective ways to recycle CKD and use it again in soil stabilization to avoid the failure of the entire pavement in the future as well as  
an economical and environmental solution, while there is a dearth of research done on RMMD. In this study, the performance of a weak  
subgrade for one of the sites in Aleppo city was examined, where its physical and mechanical properties (plasticity index, maximum dry  
density, optimum water content, and California bearing ratio (CBR)), were determined. Then RMMD was added to the subgrade samples  
according to five ratios 0, 5, 10, 15, and 20% of the dry weight of the soil. The research concluded that adding the RMMD to the weak  
subgrade by 20% of its dry weight is the optimal ratio, improved its performance, as the plasticity index decreased by 13%, and the CBR  
increased up to 63 %. Thus, the bearing capacity increases, it saves costs and reduces future pavement maintenance.  
Keywords: Soil Stabilization, Weak Soil, Mill Dust, Chemical additive  
1
which the bearing capacity is enhanced by compaction of the soil  
1
Introduction  
to a sufficient degree, or by means of piles or application of an  
external load on the soil or the use of good drainage of water, or  
stone columns [15, 16]. The second technique is chemical  
stabilization of soil by a chemical reaction between weak soils  
and the added active substance [17, 18]. Among these materials  
are lime, gypsum, cement, asphalt, resin, fly ash, and other  
materials such as industrial or natural wastes such as the CKD and  
rice husk ash [15, 19, 20, 21, 22, and 23]. The common soil  
additives are lime and cement (traditional stabilizers) [24].  
RMMD is of great importance in the field of civil engineering and  
its projects, and one of these uses is to improve weak soils. The  
flying dust is captured and collected from the raw material mill of  
the cement factory in Hama, Syria through two types of filters,  
Electrostatic and Baghouse Filters as well as for the dust flying  
throughout the entire manufacturing process of cement.  
RMMD has been chosen as a weak soil stabilizer for several  
reasons, the most important of which is its large quantities and it  
is being a completely new material in this topic of soil  
stabilization in road pavement. The fact that the total quantity of  
the electric filter of the raw material mill is large when compared  
to the Baghouse filter, the research has focused on studying its  
effect on soil performance.  
The great growth in modern buildings imposed the need for  
lands with good bearing capacity to safely withstand high  
pressures [1]. One of the important issues facing the pavement  
engineer is to provide economically viable layer thicknesses that  
are compatible with the site's soil characteristics [2, 3]. The  
general case is the lack of alternative design solutions to avoid  
weak soils, hence it is necessary to search for low-cost  
experimental alternatives [4, 5]. The weak soil has the high  
compressibility, poor shear strength, high ratio of moisture, low  
workability, which produces extra settlements of soil, and this  
makes the construction process on such soils a high probability  
issue [6]. For road pavements, soil properties have a major  
influence in determining the thickness of the layers above [7].  
Thus, road performance and service are greatly influenced by the  
stability and stiffness of the subgrade [8, 9]. Consequently, these  
soil must be stabilized or treated to increase in its geotechnical  
characteristics. the term soil stabilization is a technique in which  
weak soil properties are improved to fulfil its functions  
(
operational conditions of the road and the subsequent volumetric  
changes of soil) as the foundation for the structures based on it  
10, 11, 12, 13]. There are two techniques that are widely used for  
soil stabilization [14]. The first method is a mechanical method in  
[
Corresponding author: Fatima Alsaleh, Department of Transportation Engineering, Faculty of Civil Engineering, University of Aleppo. E-  
mail: falkhalil@meu.edu.jo  
172  
Journal of Environmental Treatment Techniques  
2021, Volume 9, Issue 1, Pages: 172-177  
Figure 1: shows the parts of the cement factory, with electrical and Baghouse filters [27]  
1
- Quarries, 2- Crushers, 3- The homogenizing process, 4- The assembly process, 5- Feed silos of the raw material mill, 6- The main  
chimney, 7- Electric and Baghouse filters, 8- The raw material mill, 9- Raw material feeding silos, 10- gas temperature adjustment tower,  
1- filters, 12- mixing chambers, 13- preheating tower (spiral), 14- raw coal, 15- coal mill, 16- filters, 17- tube cooler, 18- Electrical and  
1
Baghouse filters, 19- clinker cooler, 20- rotary kiln, 21- clinker silos, 22- gypsum / plaster, 23- assorted metals, 24- sorters, 25- cement  
mill (finishing), 26- filters, 27- packaging 28- Loading and transport platform.  
It should be noted that their physical and chemical properties  
between them are similar. Engineers strive for low-cost  
alternatives while maintaining appropriate performance, as  
materials with good specifications require high cost [25, 26].  
Figure 1 shows the parts of the Hama Cement Factory and the  
location of the electrical filter for the raw materials mill [27].  
its physical properties. There is a difference in the chemical  
composition of RMMD and CKD, and this has been proven by  
laboratory experiments, but there is a percentage of up to 48.3%  
of Cao that is somewhat close to the composition of CKD.  
1
00  
2
Methodology  
Improving the performance of the subgrade by using RMMD  
9
0
as an additive to their structure was investigated, by studying the  
effect of adding RMMD on its physical and mechanical  
properties.  
80  
7
6
5
0
0
0
2
.1 Materials used  
Subgrade materials: Soil samples from one of the sites near  
40  
the city of Aleppo were brought to the laboratory, where the  
required quantity was taken at a depth exceeding 50 cm. A grain  
size analysis, soil classification, the optimum moisture content  
3
2
1
0
0
0
0
(
OMC), shear resistance, and CBR were carried out. Table 1  
shows the characteristics of the subgrade soil. Figure 2 shows a  
grain size analysis.  
0.01  
0.1  
1
10  
100  
RMMD: It is a by-product material that is generally produced  
when grinding raw materials in the cement factory, the city of  
Hama, Syria. It has been added to soil samples according to 0, 5,  
Siev openning(mm)  
Figure 2: The soil gradation  
1
0, 15, and 20% of the dry weight of the soil. Regarding the  
chemical composition of RMMD, which was adopted as an  
additive to soil samples, it is shown in table 2, and table 3 shows  
173  
Journal of Environmental Treatment Techniques  
2021, Volume 9, Issue 1, Pages: 172-177  
Table 1: Subgrade properties  
Oven and coolant: The homogeneous raw materials are  
pulled from the bottom of the storage silo into the feed slot of a  
multi-stage primary heating tower, and the tower may reach a  
height of 280 m. Natural gas or diesel oil is used as a source of  
heat energy, and hot air from clinker cooling is used as an  
additional source of heat. The kiln is tilted slightly on the  
horizontal plane to allow a slow movement of solids down, so the  
distance is cut to the feed hole at the top of the oven to the lower  
end (combustion) where high-temperature combustion gases are  
generated in a period of 1 to 3 hours, while Combustion gases  
move upward in the current opposite to the movement of solids.  
The hot combustion gases heat the raw materials at the oven feed  
slot and provide calcium carbonate [28][29].  
Properties  
Value  
Clay and silt%  
Sand%  
28.6%  
Grain Size  
Analysis  
57.88%  
13.52%  
Gravel%  
LL%, liquid limit,  
ASTM D 4318  
PL% ,plasticity limit,  
ASTM D 4318  
4
2
2
3
Atterberg  
Limits  
PI% (plasticity index)  
19  
3
MDD (gr/cm ) ASTM D 698  
1.72  
Modified  
Proctor  
Final milling and packing: The clinker is transported to  
special mills, where the gypsum is added to it and the product is  
packed in bags to be exported and marketed [28].  
OMC %, ASTM D 698  
17.8  
USCS, ASTM D 2487  
AASHTO  
SC  
Soil  
Classification  
A-2-7  
10.5 %  
3 Results and discussion  
3
.1 Plasticity characteristics (LL, PL, PI)  
The effects of adding RMMD on LL, PL, and PI of soil are  
CBR, ASTM D1883-05  
shown in Figure 3. The LL and PL decline with the addition of  
RMMD. This may be attributed to Cationic interchange of soil  
units with calcium ions which leads to drop LL because of  
suppression of flocculated clay clusters (this decreases the soil's  
attraction to water) [30, 31], which, in turn, decreases in the PI of  
subgrade soil. A decrease in PI is a clear indication of  
improvement of soil physical properties as it increases  
workability [21]. The best PI decrease was reached at 20%  
RMMD, the largest decrease in PI was at 20% RMMD, dropping  
from 19 for subgrade soils to 15 for stabilized soil. In this regard,  
a relationship between the PI and the percentages of RMMD for  
the subgrade soil can be presented, as shown in Figure 4.  
Table 2: Chemical composition of RMMD  
Composition  
percent  
38.47  
7.47  
PF  
SiO  
Al  
Fe  
2
2
O
3
2.65  
2
O
3
1.42  
MgO  
CaO  
Total  
L.S.F  
S.M  
1.48  
48.30  
99.78  
193.51  
1.84  
4
4
3
3
2
2
5.0  
0.0  
5.0  
0.0  
5.0  
0.0  
PI LL PL  
A.M  
1.86  
Table3: Physical properties of RMMD  
Properties  
Value  
2.69  
15.0  
0.0  
1
Specific gravity, ASTM D 854  
5
0
.0  
.0  
2
Specific surface (cm /gr)  
Moisture %, ASTM D 698  
7812  
0.7  
0
5
10  
15  
20  
RMMD %  
2
.2 Main processes in the operating line of the cement industry  
Figure 3: LL, PL, and PI changes versus RMMD %  
Crushing and mixing of raw materials:  
Raw materials of limestone, silicates, clays and surface dust  
are crushed by milling mechanisms, then sifted and transported,  
to be stored as piles in open or covered areas [28].  
3.2 Compaction characteristics (MDD, OMC)  
Figure 5 shows the general behavior of the subgrade soil, a  
gradual increase in the moisture content leads to increase the dry  
density up to maximum value, and then begins to decrease, and  
this is true for all RMMD ratios. OMC and MDD can be inferred  
for each addition of RMMD, Figure 6, 7 illustrate the relationship  
between the RMMD% and OMC and MDD. An increase in MDD  
value was observed, and this is an indication of improved  
subgrade characteristics. The mechanism of the increase can be  
explained by the effect of both the fineness of the RMMD and  
specific surface of the RMMD and flocculation. The more fine-  
grained of RMMD was able to fill larger spaces of soil whereas  
Milling: Raw materials are introduced into a rotary dryer (in  
case the moisture is more than a certain percentage), where they  
are dried by hot air, then the raw materials are crushed in raw  
materials mills and transferred to pre-mixing storage silos, where  
they become homogeneous through compacting and drawing  
process, then the homogeneous raw materials are transferred from  
storage silos or other types from pre-mixing storage places to  
mixing places. The process of blending is 30% of clay, and 70%  
of limestone [28]  
174  
Journal of Environmental Treatment Techniques  
2021, Volume 9, Issue 1, Pages: 172-177  
the higher specific surface of the RMMD to the soil encouraged  
MDD increase.  
to an increase in the bearing capacity of the soil, as different  
studies have shown that the creation of calcium hydroxide  
(
Ca(OH)2) produced during the process of hydration of RMMD  
with water, this hydrate compound absorbed by the clay unites  
help to stabilize flocculated fine clay, as a result the adjustment  
of the clay microstructure has been occurred [21].  
PI= -0.0013(RMMD)2 - 0.0749(RMMD) + 17.85  
1
1
1
1
1
1
1
8.0  
7.5  
7.0  
6.5  
6.0  
5.5  
5.0  
R² = 0.9769  
MDD = 0.000003(RMMD)2 + 0.0022(RMMD) + 1.7229  
1
1
1
1
1
.79  
.78  
.77  
.76  
.75  
R² = 0.9526  
1.74  
0
5
10  
RMMD %  
Figure 4: The relationship between the PI and RMMD %  
15  
20  
1
1
1
.73  
.72  
.71  
0
5
10  
15  
20  
RMMD %  
REMF0  
REMF5  
REMF10  
REMF15  
REMF20  
Figure 7: MDD according to the RMMD%  
1
1
1
1
1
1
1
1
1
1
1
1
1
.84  
.82  
.80  
.78  
.76  
.74  
.72  
.70  
.68  
.66  
.64  
.62  
.60  
CBR = 0.0186RMMD2 - 0.0094RMMD+  
10.369  
19  
R² = 0.9  
1
1
1
8
7
6
15  
14  
13  
12  
11  
10  
9
8
1
0
12  
14  
16  
18  
20  
Moisture content %  
Figure 5: variations of dry density of subgrade soil according to  
the moisture content and RMMD%  
0
5
10  
15  
20  
RMMD %  
OMC = -0.0014(RMMD)2 - 0.0734(RMMD) + 17.849  
1
1
1
1
1
1
8.0  
7.5  
7.0  
6.5  
6.0  
5.5  
R² = 0.9772  
Figure 8: CBR according to the RMMD%  
Increase in the CBR of modified samples by the RMD  
considered a sustainable solution to the problem of solid waste  
harmful to the environment [34, 35].  
3
Conclusion  
Based on the investigations carried out in this research,  
RMMD can be considered a soil stabilizer, as its use improves the  
mechanical and physical properties of subgrade soil. The CBR  
value increased up to 63% when adding 20% of the RMMD  
compared to the reference samples (0% of the RMMD). The  
plasticity index of the soil decreased by 13% when adding 20%  
of RMMD. Furthermore, MDD increases with an increase  
RMMD ratio, and the OMC value decreases as the RMMD ratio  
increases. In addition to the above, the use of RMMD in soil  
stabilization constitutes a new scientific start for researchers to  
explore other soil properties. It is also considered sustainable  
sources of low-cost additives (reducing the thickness of road  
layers) and using these materials in soil stabilization will preserve  
the environment from harmful effects.  
0
5
10  
RMMD %  
Figure 6: OMC % according to the RMMD%  
15  
20  
3
.3 Mechanical properties (CBR)  
The CBR test is performed to calculate the bearing capacity  
of the subgrade or base course of highway pavement [32, 33].The  
CBR experiment was conducted with consideration of the OMC  
corresponding to the MDD for each of the samples (0, 5, 10, 15,  
and 20 % of RMMD). The samples were submerged in water for  
days to suit the most dangerous situation. The CBR value have  
been increased 64 % at adding 20% of RDDM as shown in Figure  
. This indicates that increasing the percentage of RMMD leads  
7
8
175  
Journal of Environmental Treatment Techniques  
2021, Volume 9, Issue 1, Pages: 172-177  
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Aknowledgment  
The researchers thank very much to the Faculty of Civil  
Engineering at the University of Aleppo and Hama Cement  
Factory for their support in carrying out the laboratory  
experiments for this work. The authors are grateful to the Middle  
East University, Amman, Jordan for the financial support granted  
to cover the publication fee of this research article.  
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Ethical issue  
Authors are aware of, and comply with, best practice in  
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(
avoidance of guest authorship), dual submission, and  
manipulation of figures, competing interests and compliance with  
policies on research ethics. Authors adhere to publication  
requirements that submitted work is original and has not been  
published elsewhere in any language.  
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Competing interests  
The authors declare that there is no conflict of interest that  
would prejudice the impartiality of this scientific work.  
1
[
2
Authors’ contribution  
[19]Emmanuel, E., Paris, M., & Deneele, D. (2019). Insights on the clay  
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All authors of this study have a complete contribution for data  
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[
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of Using Industrial Wastes for Production of Geopolymer Binder as  
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